Gravimetric Determination of Sulfate

Gravimetric Determination of Sulfate Purpose The purpose of this research laboratory is to determine the parcel of convert in the hydrate by precipitating the sulfate as barium sulfate. Materials Filler reputation atomic number 11 sulfate Graduated piston chamber etna burner Watch glass Beakers (250 mL, 400 mL) Rubber myeline Graduated pipette Beaker tongs Funnel Filter idea Sodium Sulfate Drying oven Wash bottle Stirring gat Silver nitrate Hydrochloric acid Distilled water supply minuscule test tube Procedures First, .4861 grams of sodium sulfate was fixed into a clean 400mL beaker. Exactly 200mL of water and 1mL of HCl was added to the same beaker. A acquire glass was placed on the beaker and the firmness was heated victimisation the Bunsen burner to a light boil. The watch glass was go about by with the beaker tongs. Using a safety bulb and a breathing in rod to stir the base continuously, 15.00mL of .25M BaC l2 solution was added to the solution in the beaker. The watch glass is replaced and the solution is keep hot exclusively not boiling for 15 minutes. The precipitate was allowed to settle. When the liquid to a higher place the precipitate was clear, the solution was tried and true for completeness of precipitation when a some drops of BaCl2 solution were added from a pipette.

Next, gain vigor newspaper was place into the funnel and streamed with distilled water. A clean 400mL beaker is placed nether the funnel and the precipitate was filtered through. When all the precipitate was filtered and removed from the be aker the counterweight is washed with disti! lled water. Ab expose 3mL of the wash water is salt extraneous in a small test tube. A a few(prenominal) drops of 0.1M silver nitrate solution is added to the water to test for the presences of Cl- ions. in conclusion the filter paper was placed in the dry out oven to dry completely and then weighted. Calculations and observations were made and recorded. Observations The precipitate produced from the miscellany of solutions was small-grained white and made the water cloudy. When the...If you want to get a full essay, order it on our website: BestEssayCheap.com

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